Authors:
Telepchak, Michael J. (United Chemical Technologies, Inc., Bristol, PA)
Chaney, Robert (United Chemical Technologies, Inc., Bristol, PA)
August, Thomas F. (United Chemical Technologies, Inc., Bristol, PA)
The recently published Forensic and Clinical Applications of Solid Phase Extraction, by Michael J. Telepchak, Thomas August and Glynn Chaney, has been met with enthusiasm by those in the SPE field, and has been recommended as a valuable laboratory reference. Dr. Terry Danielson, Ph.D., who reviewed the book for the American Society of Crime Laboratory Directors, calls attention to the “extensive details of many currently available SPE separation procedures,” and describes the book as a convenient compendium of SPE technology, and is relevant to the development, implementation and practice of modern SPE appropriate to students, and experienced practitioners.”
1. Introduction to Solid Phase Extraction, pp.1-40
2. Silica-Based Solid Phase Extraction, pp.41-54
3. The Chemistry of Bonded Silicas, pp.55-62
4. Bonded Phase Sorbent Synthesis, pp.63-90
5. Strategies for the Use of Solid Phase Extraction, pp.91-108
6. Optimizing Solid Phase Extraction Methods, pp.109-128
7. Separation of Analytes from Their Matrices, pp.129-146
8. Solid Phase Extraction Troubleshooting, pp.147-168
9. Drug Methods for the Toxicology Lab, pp.169-244
10. Selected Solid Phase Extraction Applications in Drug Analysis, pp.245-280
11. General Methods for Drug Isolation, pp.281-296
12. Chemical Derivatization, pp.297-310
Appendix A: Glossary, pp.311-314
Appendix B: Reagents, pp.315-316
Appendix C: Preparation of Solutions and Buffers, pp.317-320
Appendix D: Milliequivalent and Millimol Calculations, pp.321-322
Appendix E: Selected Solvent Polarity and Property Scale, pp.323-324
Appendix F: Buffers for Solid Phase Extraction, pp.325-326
Appendix G: pKa Reference for Solid Phase Extraction, pp.327-334
Appendix H: Rapid Trace® Operating Guide, pp.335-342
Appendix I: Further Reading, pp.343-350
Index: pp.351-370
Abstract:
This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.
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Artikelnummer: |
ZZ3801 |
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Preis: |
120,- Euro |